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NEW STRATEGIES FOR HYDROSILYLATION OF PROPARGYL ALCOHOLS, OLEFIN POLYMERIZATION AND ON-CHIP ORGANIC SYNTHESIS
(2020-08-11)
The research described in this dissertation is on three different projects namely i) design and synthesis of traceless hydrosilyl acetal-directed, exo-syn hydrosilylation of propargyl alcohols to produce α-hydroxy ...
SYNTHESIS, STUDY, AND APPLICATIONS OF HIGHLY FLUORINATED COPPER PYRAZOLATE COMPLEXES OF SMALL ALKENE, ALKYNES AND CARBON MONOXIDE
(2020-07-17)
Trinuclear copper pyrazolate complexes (copper trimers) function as excellent precursors to synthesize multinuclear complexes of copper. Using highly fluorinated pyrazolates as supporting ligands, we have successfully ...
NOVEL DETECTION METHODS AND GAS-FREE HYDROXIDE ELUENT GENERATOR FOR CAPILLARY LIQUID/ION CHROMATOGRAPHY
(2020-06-17)
The light absorbed by a molecule, except for an efficient fluorophore, is mostly converted into heat, thereby causing a change in temperature. In a liquid flow system, this change in temperature results in changes in the ...
Strategies for enhancing chromatographic efficiencies in chiral and achiral supercritical and liquid chromatography
(2020-09-01)
The fundamental aim of chromatography has been to achieve baseline separation between the components of a mixture in the shortest possible time. Recently there has been a shift in the chromatographic focus of enantiomeric ...
DEVELOPMENT OF HPLC STATIONARY PHASES WITH UNIQUE SELECTIVITIES AND INTRODUCTION OF MOLECULAR ROTATIONAL RESONANCE SPECTROSCOPY IN GAS CHROMATOGRAPHY
(2020-11-23)
This thesis contributes to advancing liquid and gas chromatography by introducing new stationary phases for HPLC and a new hyphenated GC technique. In the first section, new pH stable stationary phases based on geopolymers ...
ELECTROCHEMICAL AND PHOTOELECTROCHEMICAL PROPERTIES OF OXIDE AND CHALCOGENIDE SEMICONDUCTORS
(2020-12-08)
Photoelectrochemical (PEC) water splitting via inorganic semiconductors has shown interest in technical applications such as harvesting sunlight as sustainable fuels. Chalcogen-based (S, Se, Te) semiconductors are important ...